Trace Moisture Gas Standards Generators
Trace concentration moisture is an extremely important parameter in
gases used in a wide range of processes. But there is no absolute
analytical method that can be used in all applications.
For most
sensing methods, the response to moisture is affected by the background
gas and most current methods are subject to
“poisoning” by certain contaminants. Basically, all
trace moisture sensing systems require calibration to external
standards and they must be frequently challenged with standards to
demonstrate continued accuracy.
The KIN-TEK Span Pac™ H
2O Instrument Series [
brochure] provides an economical solution to every moisture
calibration problem.
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Span Pac H20 Instrument Series -
Trace Moisture Gas Standards
- H2O concentration adjustable
over 10:1 range with single oven; 100:1 with dual oven
- High ppm to 0.1 ppm H2O range
- Welded models (W series) can go down to about 10 ppb H2O
- Industrial models have NEMA 4 cabinets and optional
purge capability
- Simple to operate
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Click here to see our
Trace Moisture Gas Standards models.
Overview
There are three special problems associated with
trace moisture calibration:
- At the lowest concentration levels, there is no real zero
reference
point for moisture. Standards prepared by simply adding water vapor to
a dry gas actually have unknown uncertainty.
- Water interacts readily with almost all materials, so
changes in
pressure or temperature can appear as transient concentration changes
and may take a very long time to stabilize.
- Water is pervasive in our atmosphere, so even the most
accurate
standard may be contaminaed in the delivery process.
The Span Pac™ H
2O systems
work on a differential principal. Calibration is based on the change in
analyzer response caused by the addition of a known water vapor
concentration from a Trace Source™ H
20
permeation tube to a
flowing stream of background gas (which may also contain some
moisture). This differential method overcomes the "no zero”
problem, and the problem of the background gas
affecting the response. Water vapor flow from the permeation tube is
measured gravimetrically, and is traceable to NIST. This technique
provides a close approximation to a primary standard, even in
situations where primary standards are not available.
Special care in design, construction and choice of components
minimizes errors due to atmospheric contamination and interactions with
other materials in the system.
As listed below, several Span Pac™ H
2O
models
are offered to insure an economical solution to every moisture
calibration problem.
Span Pac™ 61-H2O and
261-H2O
(Single & Dual Oven Models)
These single and dual-oven instruments are the basic H
2O
models. The 61-H
2O single-oven
model can produce concentrations over a 10:1
range and from over 1000 ppm down to 0.1 ppm in nitrogen and other
inert background gases. The dual-oven 261-H
2O
model that
can generate a concentration range of 100:1. An internal
purge of dry gas
is used to minimize contamination from atmospheric moisture in low
concentration service.
Span Pac™ 61-W-H2O
and 261-W-H2O
(Welded Instruments)
The welded (W) single-oven instrument is used where
the minimum
concentration required is below 0.1 ppm (100 ppb). These systems are
used
for concentrations down to about 10 ppb in inert background gases. (The
minimum concentration is actually set by the minimum practical
permeation rate.) They feature all electropolished 361L seamless
stainless steel tubing, orbitally-welded
joints, VCR®
connections at service access points and special
components for high purity service.
Span Pac ™ 61-W-H2O-SD
(Welded with
Secondary Dilution)
The welded single-oven instrument with secondary dilution (SD) is our
most
versatile moisture system. This instrument provides an internal
secondary dilution step that allows addition
of extremely low concentrations, production of a very wide
concentration range (up to 20,000:1), and the production of variable
concentrations in a fixed total flow.
Reactive Gases Model (Span Pac ™ 61-R-H2O )
The reactive gases (R) model is used to produce moisture
standards
in
reactive gases.
Industrial-grade Models
(Span Pac 61-I-H20 and 261-I-H20)
Single and dual-oven industrial-grade (I) models are available in NEMA
4
cabinets for use in harsh, nonhazardous environments. These units
contain all electropolished 316L seamless stainless steel tubing.
Optional capabilities include X-purge for Class 1, Group C or D,
Division I, or Z-purge for Class 1, Group C or D, Division II.